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Normas DIN – AENOR
DIN EN 17299:2019-12

DIN EN 17299:2019-12

Animal feeding stuffs: Methods of sampling and analysis - Screening and determination of authorized coccidiostats at additive and 1 % and 3 % cross-contamination level, and of non-registered coccidiostats and of one antibiotic at sub-additive levels, in compound feed with High Performance Liquid Chromatography - Tandem Mass Spectrometry detection (LC-MS/MS); German version EN 17299:2019

Aliments des animaux: Méthodes d'échantillonnage et d'analyse - Recherche et dosage dans des aliments composés pour animaux des coccidiostatiques autorisés aux taux d'additif et de contamination croisée à 1 % et 3 %, de coccidiostatiques non enregistrés et d'un antibiotique aux taux sub-additifs, par chromatographie en phase liquide à haute performance couplée à une détection par spectrométrie de masse en tandem (CL-SM/SM); Version allemande EN 17299:2019

Futtermittel - Probenahme- und Untersuchungsverfahren - Screening und Bestimmung von zugelassenen Kokzidiostatika in Konzentrationen von Zusatzstoffen und deren Verschleppungen im Bereich von 1 % und 3 % sowie von nicht registrierten Kokzidiostatika und von einem Antibiotikum in Konzentrationen unterhalb von Zusatzstoffen in Mischfuttermitteln mittels Hochleistungs-Flüssigchromatographie mit Tandem-Massenspektrometrie-Nachweis (LC-MS/MS); Deutsche Fassung EN 17299:2019

Fecha:
2019-12 /Active
Equivalencias internacionales:

EN 17299 (2019-08)

Relación con otras normas DIN:

Reemplaza a: DIN EN 17299:2018-09

Resumen:
This European Standard specifies a high performance liquid chromatographic - tandem mass spectrometry (HPLC-MS/MS) method for the simultaneous screening and/or determination of the eleven authorized coccidiostats (halofuginone hydrobromide, robenidine hydrochloride, nicarbazin, diclazuril, decoquinate, monensin sodium, salinomycin sodium, narasin, lasalocid A sodium, semduramicin sodium and maduramicin ammonium alpha) contents in compound feeds and feed materials of plant origin at additive and cross-contamination levels and of the five non-registered coccidiostats (ethopabate, clopidol, ronidazole, dimetridazole and amprolium) at sub-additive levels and for the screening of the prohibited furazolidone antibiotic at sub-additive level, in the same matrices. It has been fully validated only for poultry, cattle and pig compound feeds. The range of application of the method is fit for the purpose of the screening and determination of all eleven registered coccidiostats at the values set by European legislation, of the non-registered coccidiostats and of the screening of the banned antibiotic.
Keywords:
Active substances, Additives, Amprolium, Animal feed, Antibiotics, Bovines, Concentration, Decoquinate, Definitions, Determination, Determination of content, Diclazurile, Ethopabates, Furazolidone, Halofuginon, High capacity, High performance liquid chromatography, HPLC, Investigation methods, Investigations, Liquid chromatography, Mass spectrometry, Mixed animal fodder, Mixed provenders, Nicarbazine, Parasites, Pigs, Poultry, Robenidine, Sampling methods, Semduramicin, Sodium, Testing
119,63
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