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Normas DIN – AENOR
DIN EN ISO 22959:2007-12

DIN EN ISO 22959:2007-12

Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons by on-line donor acceptor complex chromatography and HPLC with fluorescence detection (ISO/DIS 22959:2007); German version prEN ISO 22959:2007

Corps gras d'origines animale et végétale - Détermination de la teneur en hydrocarbures aromatiques polycycliques par chromatographie de complexe donneur-accepteur et CLHP avec détection par fluorescence (ISO/DIS 22959:2007); Version allemande prEN ISO 22959:2007

Tierische und pflanzliche Fette und Öle - Bestimmung polycyclischer aromatischer Kohlenwasserstoffe durch direkte Donor-Akzeptor-Komplex-Chromatographie und HPLC mit Fluoreszenzdetektion (ISO/DIS 22959:2007); Deutsche Fassung prEN ISO 22959:2007

Fecha Anulación:
2019-10 /Withdrawn
Equivalencias internacionales:

ISO/DIS 22959 (2007-09)

prEN ISO 22959 (2007-09)

Relación con otras normas DIN:

Reemplazada por: DIN EN ISO 22959:2009-10

Resumen:
This method describes a high performance liquid chromatographic procedure for the determination of polycyclic aromatic hydrocarbons (PAHs) in edible fats and oils. The method has been validated for coconut (CN), olive (OV), sunflower (SF) and soyabean (BO) oil. If other oils are analysed, appropriate parameters have to be determined. The limit of quantification for the PAHs is 0,1 µg/kg. The lowest possible amount of each PAH, which can be distinguished from the baseline noise has not been determined. The validated concentration range of the method is 0,1 µg/kg to 3,5 µg/kg for each individual PAH. If it is expected that the level of the (light) PAHs in samples to be analysed will be more than 3,5 µg/kg, these samples have to be diluted before analysis. It is also possible to adjust the range of the calibration curves. However ranges exceeding 3,5 µg/kg have not been validated. PAHs which can be determined by this method are: Anthracene, Phenanthrene, Fluoranthene, Pyrene, Chrysene, 1,2-Benzanthracene, Benz(e)pyrene, Benz(a)pyrene, Perylene, 1,12-Benzperylene, Anthanthrene, 1,2,5,6-Dibenzanthracene, Coronene, Indeno(123-cd)pyrene, Benz(a)fluoranthene, Benz(b)fluoranthene, Benz(k)fluoranthene.
Keywords:
Analysis, Animal fats, Animal oils, Coconut oil, Definitions, Determination, Determination of content, Fats, Fluorimetry, Food chemistry, High performance liquid chromatography, HPLC, Hydrocarbons, Inter-laboratory tests, Liquid chromatography, Oils, Olive oil, PAH, PAK, Polynuclear aromatic hydrocarbons, Soya bean oil, Sunflower seed oil, Testing, Testing devices, Vegetable fats
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