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Normas ASTM – AENOR
ASTM D7883-19

ASTM D7883-19

Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Weak Anion Exchange High Performance Liquid Chromatography

Fecha:
2020-12-02 /Historical
Superseeded by:
Significance and Use:

4.1 The presence of 4-CBA and p-TOL in PTA used for the production of polyester is undesirable because they can slow down the polymerization process, and 4-CBA is also imparting coloration to the polymer due to thermal instability.

4.2 Determining the amount of 4-CBA and p-TOL remaining from the manufacture of PTA is often required. This test method is suitable for setting specifications and could be used as an internal quality control tool where these products are produced or are used.

Scope:

1.1 This test method2 covers the determination of the 4-Carboxybenzaldehyde (4-CBA) and p-Toluic acid (p-TOL) in purified terephthalic acid (PTA) by weak anion exchange high performance liquid chromatography (HPLC). This method is applicable for 4-CBA from 2 to 500 mg/kg and for p-TOL from 10 to 500 mg/kg, respectively.

1.2 In determining the conformance of the test results using this method to applicable specification, results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Keywords:
purified terephthalic acid; 4-Carboxybenzaldehyde; <emph type="ital">p</emph>-Toluic acid; high performance liquid chromatograph; weak anion exchange HPLC;
51,52
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