Standard Test Method for Young's Modulus, Shear Modulus, and Poisson's Ratio For Ceramic Whitewares by Resonance
1.1 This test method covers the determination of the elastic properties of ceramic whiteware materials. Specimens of these materials possess specific mechanical resonance frequencies which are defined by the elastic moduli, density, and geometry of the test specimen. Therefore the elastic properties of a material can be computed if the geometry, density, and mechanical resonance frequencies of a suitable test specimen of that material can be measured. Young's modulus is determined using the resonance frequency in the flexural mode of vibration. The shear modulus, or modulus of rigidity, is found using torsional resonance vibrations. Young's modulus and shear modulus are used to compute Poisson's ratio, the factor of lateral contraction.
1.2 All ceramic whiteware materials that are elastic, homogeneous, and isotropic may be tested by this test method. This test method is not satisfactory for specimens that have cracks or voids that represent inhomogeneities in the material; neither is it satisfactory when these materials cannot be prepared in a suitable geometry.
1.3 A cryogenic cabinet and high-temperature furnace are described for measuring the elastic moduli as a function of temperature from -195°C to 1200°C.
1.4 Modification of the test for use in quality control is possible. A range of acceptable resonance frequencies is determined for a piece with a particular geometry and density. Any specimen with a frequency response falling outside this frequency range is rejected. The actual modulus of each piece need not be determined as long as the limits of the selected frequency range are known to include the resonance frequency that the piece must possess if its geometry and density are within specified tolerances.
1.5 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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